5-Methylthio-6-trifluoromethyl-1-(3-carboxy Phenyl Carbamoyl)indoline → HCID 18005141, Verbindung

HRID 1740808

Reaktionsgleichung

Reaktionsgleichung von HRID 1740808
CSC1C=C2C(=CC=1C(F)(F)F)N(C(=O)NC1C=CC=C(C(O)=O)C=1)CC2.[CH3:28][S:29][C:30]1[CH:31]=[C:32]2[C:36](=[CH:37][C:38]=1[C:39]([F:42])([F:41])[F:40])[N:35]([C:43](=[O:56])[NH:44][C:45]1[CH:50]=[CH:49][C:48]([C:51]([O:53]CC)=[O:52])=[CH:47][CH:46]=1)[CH2:34][CH2:33]2>>[CH3:28][S:29][C:30]1[CH:31]=[C:32]2[C:36](=[CH:37][C:38]=1[C:39]([F:40])([F:41])[F:42])[N:35]([C:43](=[O:56])[NH:44][C:45]1[CH:50]=[CH:49][C:48]([C:51]([OH:53])=[O:52])=[CH:47][CH:46]=1)[CH2:34][CH2:33]2

Komponenten

3

Edukt 2

HCID 180051075-Methylthio-6-trifluoromethyl-1-(3-carboxy Phenyl Carbamoyl)indolineHCID 18005113HCID 18005113, Verbindung

Produkt 1

HCID 18005141HCID 18005141, VerbindungAusbeute 88 %

Versuchsvorschrift

This was made in the same manner as 5-methylthio-6-trifluoromethyl-1-(3-carboxy phenyl carbamoyl)indoline using 5-methylthio-6-trifluoromethyl-1-(4-ethoxycarbonyl phenyl carbamoyl)indoline to give the product as a pale green solid (2.455 g, 88%), mp>200° C.

Quellen und Nachweise

ORD-Eintrag
ord-92907de7e6ff406582e05e466881471e
Quelldatensatz
uspto-grants-1999_10
Patentnummer
US05972937

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