HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
6,11-Dihydro-2-methyldibenz[b,e]-oxepin-11-carboxylic acid → 6,11-Dihydro-N-(2,6-diisopropyl-4-thiocyanatophenyl)-2-methyldibenz[b,e]oxepin-11-carboxamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 6,11-Dihydro-2-methyldibenz[b,e]-oxepin-11-carboxylic acid | HCID 10106342 | — |
| Edukt | 4-Amino-3,5-di(propan-2-yl)phenyl thiocyanate | HCID 18998488 | — |
| Produkt | 6,11-Dihydro-N-(2,6-diisopropyl-4-thiocyanatophenyl)-2-methyldibenz[b,e]oxepin-11-carboxamide | HCID 18998484 | 78,6% |
Reaktionsschritte
The similar procedures as in Example 1 were repeated except using 1.12 g of Compound A and 1.24 g of 2,6-diisopropyl-4-thiocyanatoaniline in place of aniline to obtain 1.63 g of Compound 31.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05340807 |
| Quelldatensatz | uspto-grants-1994_08 |
| ORD ID | ord-2bcc9b1db15a40daa15556a1a3c05b65 |
| Quellennotiz | uspto-grants-1994_08 |