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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1743280Erstellt: 25. Oktober 2026

Triethylamine → 2-Propenoic acid, 3-phenyl-

https://huagongshe.com/reaction/1743280

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktTriethylamineHCID 8471—
Edukt(R)-2-Bromo-3-phenylpropionic acidHCID 11746403—
LösungsmittelEthyl AcetateHCID 8857—
Produkt2-Propenoic acid, 3-phenyl-HCID 8784—

Reaktionsschritte

5 g of crude (2R)-2-bromo-3-phenylpropionic acid (HPLC: 92.5%) were dissolved in 20 ml of ethyl acetate and treated at room temperature with 2.7 ml of triethylamine. After a stirring time of about 150 minutes, no precipitation of the product was to be observed. An HPLC analysis of the solution showed that the (2R)-2-bromo-3-phenyl-propionic acid had reacted completely to give cinnamic acid.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07009047B2
Quelldatensatzuspto-grants-2006_03
ORD IDord-fa8f039f982e47f59386fc1d90ea5567
Quellennotizuspto-grants-2006_03