HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HCID 178486040, Verbindung → HCID 178486042, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | HCID 178486040 | HCID 178486040 | — |
| Katalysator | Platinum dioxide monohydrate | HCID 11139377 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | HCID 178486042 | HCID 178486042 | 101,4% |
Reaktionsschritte
A suspension of 3.4 g (12.72 mmol) of trans-[4-(3-Hydroxy-prop-1-ynyl)-cyclohexyl]-methyl-carbamic acid tert-butyl ester in 125 ml ethanol and 810 mg of PtO2.H2O was hydrogenated (1 atm) for 7 h. The reaction was filtered (Celite) and evaporated to give 3.5 g (quantitative) of trans-[4-(3-Hydroxy-propyl)-cyclohexyl]-methyl-carbamic acid tert-butyl ester, MS: 271 (M).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07012077B2 |
| Quelldatensatz | uspto-grants-2006_03 |
| ORD ID | ord-4408f2d9198c46c3bb7c9f84ef1f8824 |
| Quellennotiz | uspto-grants-2006_03 |