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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1744410Erstellt: 27. Oktober 2026

Ethanol → Dehydroabietic Acid

https://huagongshe.com/reaction/1744410

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktEthanolHCID 702—
EduktMethanolHCID 887—
EduktAbietic AcidHCID 10569—
EduktHydroxypropyleneHCID 143500—
KatalysatorPalladiumHCID 23938—
LösungsmittelAcetic AcidHCID 176—
LösungsmittelBenzeneHCID 241—
ProduktDehydroabietic AcidHCID 94391—

Reaktionsschritte

said abietic acid at 200–300° C. for 1–5 hours with the catalyst of 0.1–5% (wt) of 5%–10% palladium/carbon, or incubating directly at 220–380° C. After incubation and cooling down, adding 0.5 to 10-fold (volume) solvent, said solvent can be any one of methanol, ethanol, propenol, acetyester acetic acid, benzene and methbenzene, keeping refluxed for 1–3 hours, filtering when it is warm, cooling down, allowing it to stand for overnight and be crystallized. Dehydroabietic acid is obtained after filtering.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07015343B2
Quelldatensatzuspto-grants-2006_03
ORD IDord-a674de46ce834a52b48eb19e4e6e755e
Quellennotizuspto-grants-2006_03