2,2-Dimethyl-6-(3-nitro-phenyl)-[1,3]dioxin-4-one → HCID 86588047, Verbindung

HRID 1745621Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1745621
[C:1]([O:5][C:6](=[O:22])[NH:7][C:8]1[CH:13]=[CH:12][C:11]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=2[F:20])=[CH:10][C:9]=1[NH2:21])([CH3:4])([CH3:3])[CH3:2].CC1(C)[O:29][C:28](=O)[CH:27]=[C:26]([C:31]2[CH:36]=[CH:35][CH:34]=[C:33]([N+:37]([O-:39])=[O:38])[CH:32]=2)[O:25]1>>[C:1]([O:5][C:6](=[O:22])[NH:7][C:8]1[CH:13]=[CH:12][C:11]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=2[F:20])=[CH:10][C:9]=1[NH:21][C:28](=[O:29])[CH2:27][C:26]([C:31]1[CH:36]=[CH:35][CH:34]=[C:33]([N+:37]([O-:39])=[O:38])[CH:32]=1)=[O:25])([CH3:4])([CH3:2])[CH3:3]

Komponenten

3

Edukt 2

HCID 222248112,2-Dimethyl-6-(3-nitro-phenyl)-[1,3]dioxin-4-oneHCID 67361423tert-Butyl (3-amino-2'-fluoro-[1,1'-biphenyl]-4-yl)carbamate

Produkt 1

HCID 86588047HCID 86588047, Verbindung

Versuchsvorschrift

Prepared from (3-amino-2′-fluoro-biphenyl-4-yl)-carbamic acid tert.-butyl ester (Example G37) and 2,2-dimethyl-6-(3-nitro-phenyl)-[1,3]dioxin-4-one (Example J12) according to the general procedure K. Obtained as a yellow solid (113 mg).

Quellen und Nachweise

ORD-Eintrag
ord-8d798fbac0e54073bd5cbef774a71820
Quelldatensatz
uspto-grants-2006_03
Patentnummer
US07018998B2

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