Hydrogen Bromide → 2,3-Dimethyl-7-(o-methoxyphenacyl)pyrrolo[2,3-b]pyridine
Reaktionsgleichung
[CH3:1][C:2]1[NH:10][C:5]2=[N:6][CH:7]=[CH:8][CH:9]=[C:4]2[C:3]=1[CH3:11].[CH3:12][O:13][C:14]1[CH:23]=[CH:22][CH:21]=[CH:20][C:15]=1[C:16](=[O:19])[CH2:17]Br.Br>>[CH3:1][C:2]1[N:10]=[C:5]2[N:6]([CH2:17][C:16]([C:15]3[CH:20]=[CH:21][CH:22]=[CH:23][C:14]=3[O:13][CH3:12])=[O:19])[CH:7]=[CH:8][CH:9]=[C:4]2[C:3]=1[CH3:11]Komponenten
4
Versuchsvorschrift
The title compound was prepared on a 1 mmol scale from 2,3-dimethylpyrrolo[2,3-b]pyridine and o-methoxyphenacyl bromide in the same manner as described in example 27 yielding 244 mg (71%) pure hydrobromide as a light yellow solid.
Quellen und Nachweise
- ORD-Eintrag
- ord-ffa9b6dd3c774b4dbf54e9fb3c43fc98