HCID 14722828, Verbindung → HCID 22399592, Verbindung

HRID 1756225Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1756225
[CH:1]1([CH2:4][C:5]2[C:6]([OH:15])=[C:7]([CH:11]=[CH:12][C:13]=2[OH:14])[C:8]([NH2:10])=[O:9])[CH2:3][CH2:2]1.I[CH2:17][CH2:18][CH2:19][O:20][C:21]1[CH:34]=[CH:33][C:24]2[CH2:25][CH2:26][CH:27]([C:29]([O:31][CH3:32])=[O:30])[O:28][C:23]=2[C:22]=1[CH2:35][CH2:36][CH3:37]>>[NH2:10][C:8]([C:7]1[CH:11]=[CH:12][C:13]([O:14][CH2:17][CH2:18][CH2:19][O:20][C:21]2[CH:34]=[CH:33][C:24]3[CH:25]=[CH:26][CH:27]([C:29]([O:31][CH3:32])=[O:30])[O:28][C:23]=3[C:22]=2[CH2:35][CH2:36][CH3:37])=[C:5]([CH2:4][CH:1]2[CH2:3][CH2:2]2)[C:6]=1[OH:15])=[O:9]

Komponenten

3

Edukt 2

HCID 14722828HCID 14722828, VerbindungHCID 15341843HCID 15341843, Verbindung

Produkt 1

HCID 22399592HCID 22399592, Verbindung

Versuchsvorschrift

The compound of Example 66 and the compound of Example 23 are reacted together under the conditions described in Example 24. The crude product is purified by chromatography on silica gel using ethyl acetate/hexane (4:6) as eluant to afford the product.

Aufarbeitung

  1. customThe crude product is purified by chromatography on silica gel
  2. customto afford the product

Quellen und Nachweise

ORD-Eintrag
ord-8295d971182e4094b23330de21466a7e
Quelldatensatz
uspto-grants-1995_08
Patentnummer
US05439937

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