HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Stannane, tributylethyl- → methyl (E) 6-(1,3-dihydro-6-ethyl-7-methyl-3-oxo-4-p-toluenesulfonyloxyisobenzofuran-5-yl)-3,4-dimethyl-4-hexenoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Stannane, tributylethyl- | HCID 88048 | — |
| Edukt | methyl (E) 6-(1,3-dihydro-7-methyl-3-oxo-4-p-toluenesulfonyloxy-6-trifluoromethanesulfonyloxyisobenzofuran-5-yl)-3,4-dimethyl-4-hexenoate | HCID 86748921 | — |
| Produkt | methyl (E) 6-(1,3-dihydro-6-ethyl-7-methyl-3-oxo-4-p-toluenesulfonyloxyisobenzofuran-5-yl)-3,4-dimethyl-4-hexenoate | HCID 86748920 | — |
Reaktionsschritte
By following the procedure of part A and substituting vinyltributyltin with ethyltributyltin, and substituting methyl (E) 6-(1,3-dihydro-7-methyl-3-oxo-4-p-toluenesulfonyloxy-6-trifluoromethanesulfonyloxyisobenzofuran-5-yl)-4-methyl-4-hexenoate with methyl (E) 6-(1,3-dihydro-7-methyl-3-oxo-4-p-toluenesulfonyloxy-6-trifluoromethanesulfonyloxyisobenzofuran-5yl)-3,4-dimethyl-4-hexenoate, there is obtained methyl (E) 6-(1,3-dihydro-6-ethyl-7-methyl-3-oxo-4-p-toluenesulfonyloxyisobenzofuran-5-yl)-3,4-dimethyl-4-hexenoate.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05444072 |
| Quelldatensatz | uspto-grants-1995_08 |
| ORD ID | ord-bc01e6cf0c1d4b5a8b5658254f514e0a |
| Quellennotiz | uspto-grants-1995_08 |