HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Bisphenol A diglycidyl ether → 2,2-Bis{4-[2-hydroxy-3-(7,7,9,9-tetramethyl-1,4-dioxa-8-azaspiro[4.5]dec-8-yl)propoxy]phenyl}propane
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Bisphenol A diglycidyl ether | HCID 2286 | — |
| Edukt | 7,7,9,9-Tetramethyl-1,4-dioxa-8-azaspiro[4.5]decane | HCID 567045 | — |
| Lösungsmittel | tert-Butanol | HCID 6386 | — |
| Produkt | 2,2-Bis{4-[2-hydroxy-3-(7,7,9,9-tetramethyl-1,4-dioxa-8-azaspiro[4.5]dec-8-yl)propoxy]phenyl}propane | HCID 20510597 | — |
Reaktionsschritte
To 50 ml of t-butanol were added 3.5 g of 2,2-bis[p-(2,3-epoxypropoxy)phenyl]propane and 5.0 g of 7,7,9,9-tetramethyl-1,4-dioxa-8-azaspiro[4.5]decane; the mixture was then reacted following the procedure described in Example 21 to give the desired Compound No. 126 in the form of a white powder having an Rf value of 0.38 on thin-layer chromatography on silica gel developed with a 20:2:1 by volume mixture of benzene, ethyl acetate and triethylamine.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04371644 |
| Quelldatensatz | uspto-grants-1983_02 |
| ORD ID | ord-13b75f9a175545c69335d2d73bc425a6 |
| Quellennotiz | uspto-grants-1983_02 |