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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1758194Erstellt: 27. Oktober 2026

Bisphenol A diglycidyl ether → 2,2-Bis{4-[2-hydroxy-3-(7,7,9,9-tetramethyl-1,4-dioxa-8-azaspiro[4.5]dec-8-yl)propoxy]phenyl}propane

https://huagongshe.com/reaction/1758194

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktBisphenol A diglycidyl etherHCID 2286—
Edukt7,7,9,9-Tetramethyl-1,4-dioxa-8-azaspiro[4.5]decaneHCID 567045—
Lösungsmitteltert-ButanolHCID 6386—
Produkt2,2-Bis{4-[2-hydroxy-3-(7,7,9,9-tetramethyl-1,4-dioxa-8-azaspiro[4.5]dec-8-yl)propoxy]phenyl}propaneHCID 20510597—

Reaktionsschritte

To 50 ml of t-butanol were added 3.5 g of 2,2-bis[p-(2,3-epoxypropoxy)phenyl]propane and 5.0 g of 7,7,9,9-tetramethyl-1,4-dioxa-8-azaspiro[4.5]decane; the mixture was then reacted following the procedure described in Example 21 to give the desired Compound No. 126 in the form of a white powder having an Rf value of 0.38 on thin-layer chromatography on silica gel developed with a 20:2:1 by volume mixture of benzene, ethyl acetate and triethylamine.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04371644
Quelldatensatzuspto-grants-1983_02
ORD IDord-13b75f9a175545c69335d2d73bc425a6
Quellennotizuspto-grants-1983_02