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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1759520Erstellt: 25. Oktober 2026

1,2-Dichloroethane → N-(1-methylethyl)-3-(4-chlorophenyl)-2-oxiranecarboxamide

https://huagongshe.com/reaction/1759520

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt1,2-DichloroethaneHCID 11—
EduktSantonoxHCID 7308—
Eduktm-Chloroperbenzoic acidHCID 70297—
EduktN-(1-methylethyl)-4-chlorocinnamoylcarboxamideHCID 53721062—
ProduktN-(1-methylethyl)-3-(4-chlorophenyl)-2-oxiranecarboxamideHCID 13041336—

Reaktionsschritte

This compound was prepared from N-(1-methylethyl)-4-chlorocinnamoylcarboxamide (18.3 g.), m-chloroperbenzoic acid (19.4 g.), 4,4'-thiobis(6-tert-butyl-m-cresol) (0.3 g.), and ethylene dichloride (250 ml.) as described in Example 7, and purified by recrystallization from ether. The compound melted at 139°-141°, and weighed 11.7 g. The analytical sample which was obtained by another recrystallization from ether melted at 143°-145°.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04341718
Quelldatensatzuspto-grants-1982_07
ORD IDord-b320f5c28d44406384b0a8cd6a627737
Quellennotizuspto-grants-1982_07