4-Fluorobenzaldehyde → HCID 22600056, Verbindung
Reaktionsgleichung
[CH3:1][S:2]([C:4]1[CH:10]=[CH:9][C:7]([NH2:8])=[CH:6][CH:5]=1)=[O:3].[F:11][C:12]1[CH:19]=[CH:18][C:15]([CH:16]=O)=[CH:14][CH:13]=1>C1C=CC=CC=1>[F:11][C:12]1[CH:19]=[CH:18][C:15]([CH:16]=[N:8][C:7]2[CH:9]=[CH:10][C:4]([S:2]([CH3:1])=[O:3])=[CH:5][CH:6]=2)=[CH:14][CH:13]=1Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
A mixture of 3.0 g (19 mmol) of 4-methylsulfinylaniline (obtained in reference example 3), 2 mL (19 mmol) of 4-fluorobenzaldehyde and 80 mL of benzene was refluxed in a Dean-Stark for 2 days. The solvent was removed and the crude product obtained was directly used in the next reaction.
Aufarbeitung
- temperaturewas refluxed in a Dean-Stark for 2 days
- customThe solvent was removed
Quellen und Nachweise
- ORD-Eintrag
- ord-4f6bba6e08f140aaba54235952f89967
- Quelldatensatz
- uspto-grants-2005_01
- Patentnummer
- US06838476B1
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