4-Nitrobenzoyl chloride → Bis-(4-nitrobenzoyl)-tripropylene glycol

HRID 1761985

Reaktionsgleichung

Reaktionsgleichung von HRID 1761985
[CH3:1][CH:2]([OH:13])[CH2:3][O:4][CH:5]([CH2:7][O:8][CH:9]([CH2:11][OH:12])[CH3:10])[CH3:6].[N+:14]([C:17]1[CH:25]=[CH:24][C:20]([C:21](Cl)=[O:22])=[CH:19][CH:18]=1)([O-:16])=[O:15]>>[N+:14]([C:17]1[CH:25]=[CH:24][C:20]([C:21]([CH:1]([C:21](=[O:22])[C:20]2[CH:19]=[CH:18][C:17]([N+:14]([O-:16])=[O:15])=[CH:25][CH:24]=2)[CH:2]([OH:13])[CH2:3][O:4][CH:5]([CH2:7][O:8][CH:9]([CH2:11][OH:12])[CH3:10])[CH3:6])=[O:22])=[CH:19][CH:18]=1)([O-:16])=[O:15]

Komponenten

3

Edukt 2

HCID 85024-Nitrobenzoyl chlorideHCID 326112-(2-(2-Hydroxypropoxy)propoxy)-1-propanol

Produkt 1

HCID 86743032Bis-(4-nitrobenzoyl)-tripropylene glycolAusbeute 89 %

Versuchsvorschrift

Tripropylene glycol (57.6 g, 0.3 mole) was treated with p-nitrobenzoyl chloride (116 g, 0.625 mole), following the general procedure described in Example 1, Part A. The product, bis-(4-nitrobenzoyl)-tripropylene glycol (131 g), was obtained as a viscous yellow oil.

Quellen und Nachweise

ORD-Eintrag
ord-3a748d601ca04ed6bc5cb8b5044b74cd
Quelldatensatz
uspto-grants-1989_05
Patentnummer
US04829099

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