Potassium Carbonate → HCID 19858315, Verbindung

HRID 1762129Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1762129
[CH3:1][O:2][CH:3]=[CH:4]C.[I:6][CH2:7][CH2:8][OH:9].[C:10](=O)([O-])[O-].[K+].[K+]>P(Cl)(Cl)(Cl)=O>[CH3:1][O:2][C:3]([O:9][CH2:8][CH2:7][I:6])([CH3:4])[CH3:10]

Komponenten

5

Edukt 3

HCID 11430Potassium CarbonateHCID 12225IodoethanolHCID 1112901-Propene, 1-methoxy-

Produkt 1

HCID 19858315HCID 19858315, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 24813Phosphorus oxychlorideKatalysator

Versuchsvorschrift

To 6 mls of cold (0° C.) methoxypropene was added 3 mls of 2-iodoethanol and 1 drop of phosphorous oxychloride (POCl3). The reaction was stirred for 1 hour and then solid potassium carbonate was added. After 10 minutes the liquid was decanted and was concentrated to obtain the product as an oil.

Aufarbeitung

  1. customAfter 10 minutes the liquid was decanted
  2. concentrationwas concentrated

Quellen und Nachweise

ORD-Eintrag
ord-42518c203af64540aaafefcd08cba9c2
Quelldatensatz
uspto-grants-1989_05
Patentnummer
US04831035

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