HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium ethanethiolate → ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-thiocarboximidate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium ethanethiolate | HCID 4459711 | — |
| Edukt | 5,7-dihydro-6H-dibenz[c,e]azepine-6carbonitrile | HCID 19833886 | — |
| Lösungsmittel | Ethanethiol | HCID 6343 | — |
| Produkt | ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-thiocarboximidate | HCID 20041719 | — |
Reaktionsschritte
starting from 5,7-dihydro-6H-dibenz[c,e]azepine-6-carbonitrile and sodium ethanethiolate in ethanethiol there is obtained ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-thiocarboximidate and therefrom with hydrochloric acid in alcohol there is obtained the hydrochloride, m.p. 220° C. (with decomposition);
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04833245 |
| Quelldatensatz | uspto-grants-1989_05 |
| ORD ID | ord-3da4a351d8e64400a8b8ced28462530c |
| Quellennotiz | uspto-grants-1989_05 |