Reaktionsgleichung
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][NH2:10])=[CH:5][CH:4]=1.[Cl:11][CH2:12][CH2:13][O:14][CH2:15][CH2:16][C:17](Cl)=[O:18]>>[Cl:11][CH2:12][CH2:13][O:14][CH2:15][CH2:16][C:17]([NH:10][CH2:9][C:6]1[CH:7]=[CH:8][C:3]([O:2][CH3:1])=[CH:4][CH:5]=1)=[O:18]Komponenten
3
Versuchsvorschrift
Title compound was prepared starting from 4-methoxyphenylmethanamine and 3-(2-chloroethoxy)propanoyl chloride following the procedure outlined for Example 27A. 1H NMR (CDCl3): δ 2.38-2.41 (m, 2H), 2.60-2.63 (m, 2H), 3.54-3.60 (m, 2H), 3.66-3.69 (m, 2H), 3.80 (s, 3H), 4.45 (d, 2H, J=6.1 Hz), 6.12 (br t, 1H, D2O exchanged), 6.80-6.87 (m, 4H).
Quellen und Nachweise
- ORD-Eintrag
- ord-c44aad0526c5420295372be403a6339b
- Quelldatensatz
- uspto-grants-2016_02
- Patentnummer
- US09260400B2
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