HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1,1'-Carbonyldiimidazole → hexahydroimidazo[1,5-a]pyridin-3(2H)-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Edukt | Piperidine-2-methylamine | HCID 90865 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | hexahydroimidazo[1,5-a]pyridin-3(2H)-one | HCID 47002315 | — |
Reaktionsschritte
A solution of CDI (830 mg, 5.1 mmol) and piperidin-2-ylmethanamine (520 mg, 4.6 mmol) in DCM (20 mL) was stirred at room temperature overnight. After the solvent was removed, the residue was directly used for the next step without further purification.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09260452B2 |
| Quelldatensatz | uspto-grants-2016_02 |
| ORD ID | ord-619ee6518b044e9c8f2128490bba4c10 |
| Quellennotiz | uspto-grants-2016_02 |