2-(Dimethoxymethyl)-1,8-naphthyridine → 2-(Dimethoxymethyl)-7-methyl-1,8-naphthyridine
Reaktionsgleichung
[NH2:1][C:2]1[N:9]=[C:8]([CH3:10])[CH:7]=[CH:6][C:3]=1[CH:4]=O.[CH3:11][O:12][CH:13]([O:24][CH3:25])[C:14]1[CH:23]=CC2C(=NC=CC=2)N=1>>[CH3:11][O:12][CH:13]([O:24][CH3:25])[C:14]1[CH:23]=[CH:4][C:3]2[C:2](=[N:9][C:8]([CH3:10])=[CH:7][CH:6]=2)[N:1]=1Komponenten
3
Versuchsvorschrift
From 2-amino-6-methylnicotinaldehyde, synthesized in an analogous manner to intermediate 5, the title compound was obtained as a white solid. (UPLC-MS 6) tR 0.62; ESI-MS 219.2 [M+H]+.
Quellen und Nachweise
- ORD-Eintrag
- ord-dc54c846cfff49169468ecad758908c6
- Quelldatensatz
- uspto-grants-2016_02
- Patentnummer
- US09266883B2
Notizen zur Reaktion
Wird geladen…