Mesitylacetic acid → Sulfamic acid[2,4,6-trimethylphenyl(acetyl)]-2,6-bis(1-methylethyl)phenyl ester

HRID 1781468

Reaktionsgleichung

Reaktionsgleichung von HRID 1781468
CC(C1C=CC=C(C(C)C)C=1C[C:14]([C:16]1[C:17]([CH:30]([CH3:32])[CH3:31])=[C:18]([O:25][S:26](=[O:29])(=[O:28])[NH2:27])[C:19]([CH:22]([CH3:24])[CH3:23])=[CH:20][CH:21]=1)=[O:15])C.C(C1C=CC=C(C(C)C)C=1CC(O)=O)(C)C.[CH3:49][C:50]1[CH:55]=[C:54]([CH3:56])[CH:53]=[C:52]([CH3:57])[C:51]=1[CH2:58]C(O)=O>>[CH3:49][C:50]1[CH:55]=[C:54]([CH3:56])[CH:53]=[C:52]([CH3:57])[C:51]=1[CH2:58][C:14]([C:16]1[C:17]([CH:30]([CH3:32])[CH3:31])=[C:18]([O:25][S:26](=[O:28])(=[O:29])[NH2:27])[C:19]([CH:22]([CH3:23])[CH3:24])=[CH:20][CH:21]=1)=[O:15]

Komponenten

4

Edukt 3

HCID 78123Mesitylacetic acidHCID 10226443Sulfamic acid[[2,6-bis(1-methylethyl)phenyl]-acetyl]-2,6-bis(1-methylethyl)phenyl esterHCID 152779902-(2,6-Diisopropylphenyl)acetic acid

Produkt 1

HCID 19046529Sulfamic acid[2,4,6-trimethylphenyl(acetyl)]-2,6-bis(1-methylethyl)phenyl ester

Versuchsvorschrift

This compound was prepared in the same manner as for the title compound of Example 1, except that 2,6-diisopropylphenylacetic acid was replaced with 2,4,6-trimethylphenylacetic acid, mp 159°-161° C.

Quellen und Nachweise

ORD-Eintrag
ord-0d049afbc8f14ed7b6fd109189e0aa58
Quelldatensatz
uspto-grants-1997_05
Patentnummer
US05633287

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