Sodium Bicarbonate → Sodium

HRID 1788622Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1788622
[N+:1]([C:4]1[CH:9]=[C:8]([N+:10]([O-:12])=[O:11])[CH:7]=[CH:6][C:5]=1CCC(O)=O)([O-:3])=[O:2].[Na:18].C(=O)([O-])O.[Na+].NC1C=C(N)C=CC=1[O:27][CH:28]([CH3:32])[C:29]([OH:31])=[O:30]>>[N+:1]([C:4]1[CH:9]=[C:8]([N+:10]([O-:12])=[O:11])[CH:7]=[CH:6][C:5]=1[O:27][CH:28]([CH3:32])[C:29]([OH:31])=[O:30])([O-:3])=[O:2].[Na:18]

Komponenten

6

Edukt 4

HCID 516892Sodium BicarbonateHCID 27505133-(2,4-dinitrophenyl)propanoic AcidHCID 5360545Sodium2×HCID 20189859HCID 20189859, Verbindung

Produkt 2

HCID 5360545SodiumHCID 20189861HCID 20189861, Verbindung

Versuchsvorschrift

The 2-(2,4-dinitrophenoxy)-propionic acid from step (a) was converted into the sodium salt with sodium hydrogen carbonate and reduced in aqueous solution, using procedures analogous to those set forth in A, and the sodium salt was then isolated. Five grams of 2-(2,4-dinitrophenoxy)-propionic acid yielded 2.4 gm of sodium salt of 2-(2,4-diaminophenoxy)-propionic acid.

Aufarbeitung

  1. customwas then isolated

Quellen und Nachweise

ORD-Eintrag
ord-0ace83c6371546509178e06bffa6169c
Quelldatensatz
uspto-grants-1987_08
Patentnummer
US04684371

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