Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Butylimidazole | HCID 61347 | — |
| Edukt | 1-(3-Bromopropyl)-4-methoxybenzene | HCID 12776996 | — |
| Produkt | HCID 178448559 | HCID 178448559 | — |
Reaktionsschritte
A mixture of 2.5 g (0.02 mole) of 1-butyl-1H-imidazole and 4.61 g (0.02 mole) of 1-(3-bromopropyl)-4-methoxybenzene is heated at 140° C. for about 1.5 hours. Follow the progress of the reaction by thin-layer chromatography on silica gel (methanol: 1M sodium chloride, 95:5). At the completion of the reaction, the cooled reaction product is triturated thoroughly with ether and on drying, provides the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US04689341 |
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| Quelldatensatz | uspto-grants-1987_08 |
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| ORD ID | ord-713fc3bc0f894dfc920890737d051b18 |
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| Quellennotiz | uspto-grants-1987_08 |
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