HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrogen Bromide → N-(4-piperidinylmethyl)-2-benzothiazolamine dihydrobromide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrogen Bromide | HCID 260 | — |
| Edukt | 1-acetyl-N-(2-benzothiazolyl)-4-piperidinemethanamine | HCID 14048944 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | N-(4-piperidinylmethyl)-2-benzothiazolamine dihydrobromide | HCID 14048948 | 79% |
Reaktionsschritte
A mixture of 140 parts of 1-acetyl-N-(2-benzothiazolyl)-4-piperidinemethanamine and 1500 parts of a hydrobromic acid solution 24% in water was stirred and refluxed for 5 hours. The reaction mixture was evaporated and the residue was suspended in boiling ethanol. After cooling, the product was filtered off and dried, yielding 122 parts (79%) of N-(4-piperidinylmethyl)-2-benzothiazolamine dihydrobromide.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04689330 |
| Quelldatensatz | uspto-grants-1987_08 |
| ORD ID | ord-c9b16aa6f74749a99eb7aab43a37c592 |
| Quellennotiz | uspto-grants-1987_08 |