HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dimethylamine → 2-Methoxy-benzylidene-dimethyl-ammonium chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dimethylamine | HCID 674 | — |
| Edukt | Acetyl chloride | HCID 6367 | — |
| Edukt | 2-Methoxybenzaldehyde | HCID 8658 | — |
| Produkt | 2-Methoxy-benzylidene-dimethyl-ammonium chloride | HCID 21985303 | — |
Reaktionsschritte
The reaction of 17.0 ml (0.135 mol) dimethylamine solution and 6.8 g (0.050 mol) 2-methoxybenzaldehyde in accordance with general synthesis instructions 1 and subsequent reaction with 3.0 ml (0.050 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 4.8 g (corresponding to 48% of the yield calculated by theory) 2-methoxy-benzylidene-dimethyl-ammonium chloride.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07034018B2 |
| Quelldatensatz | uspto-grants-2006_04 |
| ORD ID | ord-89961a47d52544488cacd38cdd5a3b89 |
| Quellennotiz | uspto-grants-2006_04 |