HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Ethynyl-6-methylpyridine → 5-Methyl-2-(6-methyl-pyridin-2-yl)-7-nitro-1h-indole
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Ethynyl-6-methylpyridine | HCID 13400635 | — |
| Edukt | 2-Iodo-4-methyl-6-nitroaniline | HCID 19735199 | — |
| Produkt | 5-Methyl-2-(6-methyl-pyridin-2-yl)-7-nitro-1h-indole | HCID 68634447 | 35,3% |
Reaktionsschritte
6-Iodo-4-methyl-2-nitroaniline (500 mg, 1.8 mmol) and 2-ethinyl-6-methylpyridine (210 mg, 1.8 mmol) were reacted according to the same procedure as Preparation 19 to give the title compound (170 mg, Yield 35%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08349885B2 |
| Quelldatensatz | uspto-grants-2013_01 |
| ORD ID | ord-e7e78dc0cebe47cfa957790382653b10 |
| Quellennotiz | uspto-grants-2013_01 |