HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → propan-2-yl (2S)-2-amino-3-phenylpropanoate hydrochloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | L-Tyrosine | HCID 6057 | — |
| Edukt | L-Phenylalanine | HCID 6140 | — |
| Lösungsmittel | Isopropanol | HCID 3776 | — |
| Produkt | propan-2-yl (2S)-2-amino-3-phenylpropanoate hydrochloride | HCID 15599949 | — |
| Produkt | propan-2-yl (2S)-2-amino-3-(4-hydroxyphenyl)propanoate hydrochloride | HCID 67262861 | — |
Reaktionsschritte
Excess HCl gas was added with stirring to a suspension of L-phenylalanine or L-tyrosine in excess isopropanol. The mixture was heated to reflux for 16 h, and then the volatiles were evaporated under vacuum to give L-phenylalanine isopropyl ester hydrochloride or L-tyrosine isopropyl ester hydrochloride of sufficient purity for immediate use.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07741328B2 |
| Quelldatensatz | uspto-grants-2010_06 |
| ORD ID | ord-733fefb0a17c4d6aa12ad2ef65fce39e |
| Quellennotiz | uspto-grants-2010_06 |