HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1814856Erstellt: 26. Oktober 2026
1-Carbethoxy-4-ethylamino-3-methylpiperidine → 4-Ethylamino-3-methylpiperidine
https://huagongshe.com/reaction/1814856
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | 1-Carbethoxy-4-ethylamino-3-methylpiperidine | HCID 22278900 | — |
| Lösungsmittel | Sodium Hydroxide | HCID 14798 | — |
| Produkt | 4-Ethylamino-3-methylpiperidine | HCID 22278859 | — |
Reaktionsschritte
1-Carbethoxy-4-ethylamino-3-methylpiperidine (2.3 g, 10.74 mmol) was suspended in 5 M NaOH solution (15 ml), stirred at 110° C. for 120 hr, cooled, extracted with ethyl acetate, dried (Na2SO4) and concentrated to dryness to afford 4-ethylamino-3-methylpiperidine. Yield 0.7 g (46%), C8H18N2, m/z 143, (M+1).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US06878713B2 |
|---|
| Quelldatensatz | uspto-grants-2005_04 |
|---|
| ORD ID | ord-7c81572937964c84ad9ea0cf4f9f1b4a |
|---|
| Quellennotiz | uspto-grants-2005_04 |
|---|
