2-Chlorobenzaldehyde → 3'-Chloro-4'-[(2-chlorophenyl)thio]acetophenone

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Reaktionsgleichung

[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[SH:8].ClC1C=CC=CC=1C=O.F[C:19]1[CH:24]=[CH:23][C:22]([C:25](=[O:27])[CH3:26])=[CH:21][C:20]=1[Cl:28]>>[Cl:28][C:20]1[CH:21]=[C:22]([C:25](=[O:27])[CH3:26])[CH:23]=[CH:24][C:19]=1[S:8][C:3]1[CH:4]=[CH:5][CH:6]=[CH:7][C:2]=1[Cl:1]

Komponenten

Edukt 3

HCID 69962-Chlorobenzaldehyde

HCID 80599o-Chlorothiophenol

HCID 5204223'-Chloro-4'-fluoroacetophenone

Produkt 1

HCID 220231783'-Chloro-4'-[(2-chlorophenyl)thio]acetophenone

Versuchsvorschrift

The title compound was prepared by the procedures described in Example 1A substituting 2,4-dichlorothiophenol with 2-chlorothiophenol, and 2-chlorobenzaldehyde with 4′-fluoro-3′-chloroacetophenone.

Quellen und Nachweise

ORD-Eintrag: ord-9282173127c64415b0eea3ee3ba28ce7
Quelldatensatz: uspto-grants-2005_04
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US06878700B1

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