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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1815595Erstellt: 24. Oktober 2026

Methylamine → Melamine, methyl-

https://huagongshe.com/de/reaction/1815595

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktMethylamineHCID 6329—
Edukt1,3,5-Triazine-2,4-diamine, 6-chloro-HCID 18831—
ProduktMelamine, methyl-HCID 2602965%

Reaktionsschritte

A mixed solution comprising 14.5 g (0.1 mol) of 2,4-diamino-6-chloro-1,3,5-triazine synthesized in Reference Example 1 and 31.1 g (0.4 mol) of 40% aqueous solution of methylamine was heated under stirring and reacted finally at the reflux temperature thereof for 6 hours. After cooling the reacted solution, products were filtered off, and washed with cold water. The resulting filter residue was dried in vacuo at 70° C. for 6 hours to give 9.1 g (yield: 65%) of the titled compound. Malting point: 269° C.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06878824B2
Quelldatensatzuspto-grants-2005_04
ORD IDord-db82ff322d4b4ffa9331772067bb510c
Quellennotizuspto-grants-2005_04