HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methylamine → Melamine, methyl-
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methylamine | HCID 6329 | — |
| Edukt | 1,3,5-Triazine-2,4-diamine, 6-chloro- | HCID 18831 | — |
| Produkt | Melamine, methyl- | HCID 26029 | 65% |
Reaktionsschritte
A mixed solution comprising 14.5 g (0.1 mol) of 2,4-diamino-6-chloro-1,3,5-triazine synthesized in Reference Example 1 and 31.1 g (0.4 mol) of 40% aqueous solution of methylamine was heated under stirring and reacted finally at the reflux temperature thereof for 6 hours. After cooling the reacted solution, products were filtered off, and washed with cold water. The resulting filter residue was dried in vacuo at 70° C. for 6 hours to give 9.1 g (yield: 65%) of the titled compound. Malting point: 269° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06878824B2 |
| Quelldatensatz | uspto-grants-2005_04 |
| ORD ID | ord-db82ff322d4b4ffa9331772067bb510c |
| Quellennotiz | uspto-grants-2005_04 |