Allylamine → HCID 22493227, Verbindung

HRID 1816248Notizen

Reaktionsgleichung

[CH2:1]([NH:4][C:5](=[O:13])[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=1[NH2:12])[CH:2]=[CH2:3].[CH2:14]([NH2:17])[CH:15]=C.[C:18]12[C:24](=CC=CC=1)[NH:23]C(=O)OC2=O>>[CH2:1]([NH:4][C:5](=[O:13])[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=1[NH:12][CH2:15][C:14]1[NH:17][CH2:18][CH2:24][N:23]=1)[CH:2]=[CH2:3]

Komponenten

Edukt 3

HCID 7853Allylamine

HCID 8359Isatoic Anhydride

HCID 2062656N-allyl-2-aminobenzamide

Produkt 1

HCID 22493227HCID 22493227, Verbindung

Versuchsvorschrift

N-Allyl-2-amino benzamide (prepared from allylamine and isatoic anhydride, using the methods described in Example 17) and CMI were reacted using conditions described in the general procedure for CMI coupling to give N-allyl-2-[(4,5-dihydro-1H-imidazol-2-ylmethyl)amino]benzamide, isolated as the hydrochloride salt.

Aufarbeitung

customwere reacted

Quellen und Nachweise

ORD-Eintrag: ord-23dbf787be854ceebb1efbf99ca9b9cf
Quelldatensatz: uspto-grants-2005_04
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US06884801B1

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