1-Isopropylhydrazine hydrochloride → HCID 54535900, Verbindung
Reaktionsgleichung
C[N:2]([CH:4]=[N:5][C:6](=O)[C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[N+:13]([O-:15])=[O:14])C.Cl.[CH:18]([NH:21]N)([CH3:20])[CH3:19]>>[CH3:19][CH:18]([N:21]1[C:6]([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=2[N+:13]([O-:15])=[O:14])=[N:5][CH:4]=[N:2]1)[CH3:20]Komponenten
3
Versuchsvorschrift
N-[(Dimethylamino)methylene]-2-nitrobenzamide, prepared in Example 90, and isopropylhydrazine hydrochloric acid salt were reacted as in Example 90 to give 1-(2-propyl)-5-(2-nitrophenyl)-1,2,4-triazole, which was reduced and coupled with CMI similarly to give the fumaric acid salt of N-(4,5-dihydro-1H-imidazol-2-ylmethyl)-2-(2-propyl-1H-1,2,4-triazol-5-yl)aniline.
Aufarbeitung
- customwere reacted as in Example 90
Quellen und Nachweise
- ORD-Eintrag
- ord-3c39c6dfd40842ae9dde7b7797a7ba0a
- Quelldatensatz