Zurück
HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1819978Erstellt: 26. Oktober 2026

Piperonal → Bis(3,4-methylenedioxy)chalcone

https://huagongshe.com/reaction/1819978

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPiperonalHCID 8438—
EduktSodium HydroxideHCID 14798—
EduktAcetopiperoneHCID 76622—
LösungsmittelEthanolHCID 702—
ProduktBis(3,4-methylenedioxy)chalconeHCID 294346—

Reaktionsschritte

A mixture of piperonal (460 mg) and 3,4-methylenedioxyacetophenone (500 mg) in ethanol (20 ml) was treated with 1M NaOH solution (4 ml), then the mixture was stirred overnight. The pale yellow crystalline solid was filtered off, washed with water then cold aqueous ethanol and dried to give pure bis(3,4-methylenedioxy)chalcone DC-0006B (476 mg, 53%).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07601876B2
Quelldatensatzuspto-grants-2009_10
ORD IDord-398f59d5fd724c3fa100713fa1a5177c
Quellennotizuspto-grants-2009_10