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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1820742Erstellt: 26. Oktober 2026

4-Bromobenzohydrazide → 2-(4-Bromophenyl)-1,3,4-oxadiazole

https://huagongshe.com/reaction/1820742

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt4-BromobenzohydrazideHCID 22219—
EduktEthyl orthoformateHCID 31214—
Produkt2-(4-Bromophenyl)-1,3,4-oxadiazoleHCID 715120—

Reaktionsschritte

12.3 mmol of 4-bromo-benzoic acid hydrazide were dissolved in 26 ml of triethyl orthoformate. The reaction mixture was stirred overnight at 140°, evaporated and the residue crystallized from ethanol to give the title compound as a colorless solid. MS (m/e): 225.0 (MH+, 100%)

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07605163B2
Quelldatensatzuspto-grants-2009_10
ORD IDord-79989d43b7124d63ba0f90eb321aa375
Quellennotizuspto-grants-2009_10