HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethanol → N-Cyclopentyl-amino-acetic acid ethyl ester hydrochloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethanol | HCID 702 | — |
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Edukt | 2-(Cyclopentylamino)acetic acid | HCID 314101 | — |
| Produkt | N-Cyclopentyl-amino-acetic acid ethyl ester hydrochloride | HCID 13089663 | — |
Reaktionsschritte
Cyclopentylglycine ethyl ester hydrochloride salt was prepared by the procedure in Example 1(B) utilizing cyclopentylglycine (5.0 g, 38.7 mmol), thionyl chloride (6.0 mL, 77.4 mmol) and EtOH (34.10 mL, 58.1 mmol). The ethyl ester 14aj was obtained as a white solid (2.25 g, 10.86 mmol, 56%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07608599B2 |
| Quelldatensatz | uspto-grants-2009_10 |
| ORD ID | ord-3191a0ced3354e80a1eb982961fc1c18 |
| Quellennotiz | uspto-grants-2009_10 |