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Dicyclohexylcarbodiimide → HCID 21976135, Verbindung

HRID 1823187
Notizen
Druckvorschau

Reaktionsgleichung

Reaktionsgleichung von HRID 1823187
[C:1]1([CH3:21])[CH:6]=[C:5]([CH3:7])[CH:4]=[C:3]([CH3:8])[C:2]=1[N:9](C1C=CC=CC=1)[C:10](=[O:14])[C:11]([OH:13])=O.ON1C2C=CC=CC=2N=N1.C1(N=C=NC2CCCCC2)CCCCC1.[NH2:47][C:48]1[CH:53]=[C:52]([CH3:54])[CH:51]=[C:50]([C:55]([CH3:58])([CH3:57])[CH3:56])[C:49]=1[OH:59]>C1COCC1>[C:3]1([CH3:8])[CH:4]=[C:5]([CH3:7])[CH:6]=[C:1]([CH3:21])[C:2]=1[NH:9][C:10](=[O:14])[C:11]([NH:47][C:48]1[CH:53]=[C:52]([CH3:54])[CH:51]=[C:50]([C:55]([CH3:57])([CH3:56])[CH3:58])[C:49]=1[OH:59])=[O:13]
KomponentenReaktionsbedingungenVersuchsvorschriftAufarbeitungQuellen und NachweiseNotizen zur Reaktion

Komponenten

6

Edukt 4

HCID 10868DicyclohexylcarbodiimideHCID 757711-HydroxybenzotriazoleHCID 5964582-Amino-6-tert-butyl-4-methyl-phenolHCID 21976145HCID 21976145, Verbindung

Produkt 1

HCID 21976135HCID 21976135, VerbindungAusbeute 76 %

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 8028
Tetrahydrofuran
Lösungsmittel

Reaktionsbedingungen

Temperatur
0 °C

Versuchsvorschrift

N-(Mesityl)-oxanilic acid (2.15 g, 10.4 mmol, 1.0 eq), prepared according to the synthesis method described in Example 5, and 1-hydroxybenzotriazole (2.39 g, 15.6 mmol, 1.5 eq) were added to an oven dried, two-necked flask, forming a solution. THF (100 ml) was then added and the solution was cooled to 0° C. 1,3-dicyclohexylcarbodiimide (1 M in CH2Cl2) (12.5 ml, 12.5 mmol, 1.2 eq) was then added to the solution. The solution was then allowed to stir at 0° for one hour. During this time, a white precipitate formed. 2-amino-4-methyl-6-tert-butylphenol (1.863 g, 10.4 mmol, 1.0 eq), prepared according to the synthesis method described in Example 6, was then added to the suspension. The suspension was then allowed to stir overnight. The next day, the solvent was removed under reduced pressure, and ethyl acetate was added. The resulting suspension was then filtered to remove the solid. The filtrate was washed with 10% citric acid solution (2×50 ml), 5% NaHCO3 (2×50 ml) and brine (50 ml). It was dried over MgSO4, and the solvent was removed under reduced pressure, leaving a solid which was recrystallized from hexane to give the product as a white solid (2.92 g, 7.9 mmol, 76% yield). 1H NMR (300 MHz, CDCl3) δ 9.55 (s, 1H), 8.77 (s, 1H), 7.84 (s, 1H), 7.05 (d, J=1.8 Hz, 1H), 6.92 (m, 3H), 2.30 (s, 3H), 2.28 (s, 3H), 2.22 (s, 6H), 1.45 (s, 9H); 13C NMR (75 MHz, CDCl3) δ 158.5, 157.4, 146.2, 140.6, 138.1, 134.9, 129.9, 129.6, 129.4, 126.9, 124.9, 121.4, 35.3, 30.0, 21.2, 21.0, 18.5. Anal. Calcd for C22H28N2O3: C, 71.71; H, 7.66; N, 7.60. Found: C, 72.01; H, 8.03; N, 7.36.

Aufarbeitung

  1. customaccording to the synthesis method
  2. additionwere added to an oven
  3. customdried
  4. customtwo-necked flask, forming a solution
  5. customDuring this time, a white precipitate formed
  6. customaccording to the synthesis method
  7. additionwas then added to the suspension
  8. stirringto stir overnight
  9. customThe next day, the solvent was removed under reduced pressure, and ethyl acetate
  10. additionwas added
  11. filtrationThe resulting suspension was then filtered
  12. customto remove the solid
  13. washThe filtrate was washed with 10% citric acid solution (2×50 ml), 5% NaHCO3 (2×50 ml) and brine (50 ml)
  14. dry with materialIt was dried over MgSO4
  15. customthe solvent was removed under reduced pressure
  16. customleaving a solid which
  17. customwas recrystallized from hexane

Quellen und Nachweise

ORD-Eintrag
ord-10e27a2ac8d14cbaa4424769bf4f00ae
Quelldatensatz
uspto-grants-2006_05
DOI
10.6084/m9.figshare.5104873.v1
Patentnummer
US07037987B2

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