HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → 2-Bromo-1-(4-ethylphenyl)ethan-1-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | 4'-Ethylacetophenone | HCID 13642 | — |
| Edukt | Bromine | HCID 24408 | — |
| Lösungsmittel | Diethyl Ether | HCID 3283 | — |
| Lösungsmittel | Chloroform | HCID 6212 | — |
| Produkt | 2-Bromo-1-(4-ethylphenyl)ethan-1-one | HCID 12401951 | — |
Reaktionsschritte
20 mmol of 1-(4-ethylphenyl)ethan-1-one, 1 ml conc. HCl were mixed in 20 ml diethyl ether at 0° C. under nitrogen. To this solution a solution of 20 mmol Br2 in 20 ml chloroform was added drop wise and left for four hours and then concentrated in vacuo to obtain 2-bromo-1-(4-ethylphenyl)ethan-1-one.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07037918B2 |
| Quelldatensatz | uspto-grants-2006_05 |
| ORD ID | ord-1e43f89d5420435a8ce90e2af09d5fdb |
| Quellennotiz | uspto-grants-2006_05 |