4-Nitrobenzenesulfonamide → N-{3-[4-(1,2-diphenyl-but-1-enyl)-phenyl]-acryloyl}-4-nitro-benzenesulfonamide

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	4-Nitrobenzenesulfonamide	HCID 22784	—
Edukt	3-[4-(Z)-(1,2-diphenylbut-1-enyl)phenyl]-acrylic acid	HCID 3036152	—
Produkt	N-{3-[4-(1,2-diphenyl-but-1-enyl)-phenyl]-acryloyl}-4-nitro-benzenesulfonamide	HCID 69780499	—

Reaktionsschritte

Prepared by coupling 1a and 4-nitrobenzenesulfonamide in accordance with Procedure 1, Method A described hereinabove. Yield (32%); 1H NMR (d6-DMSO) δ 8.33 (d, J=8.8 Hz, 2H), 8.08 (d, J=8.8 Hz, 2H), 7.38–7.07 (m, 13H), 6.82 (d, J=8.0 Hz, 2H), 6.35 (d, J=15.7 Hz, 1H), 2.35 (q, J=7.3 Hz, 2H), 0.81 (t, J=7.3 Hz, 3H); APcI m/z: 538 (M+).

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US07045540B2
Quelldatensatz	uspto-grants-2006_05
ORD ID	ord-4ccfb4a47e9641bd98a3b6ed72586af3
Quellennotiz	uspto-grants-2006_05