HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethyl indole-2-carboxylate → 7-Fluoro-1-methylindole-3-carboxaldehyde
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethyl indole-2-carboxylate | HCID 73125 | — |
| Edukt | 7-Fluoro-1H-indole-3-carbaldehyde | HCID 22139120 | — |
| Produkt | 7-Fluoro-1-methylindole-3-carboxaldehyde | HCID 22139037 | 43% |
Reaktionsschritte
According to the procedure of Preparation 9 (a), except substituting 7-fluoro-1H-indole-3-carboxaldehyde (0.5 g, 3.1 mmole) for the ethyl indole-2-carboxylate, the title compound (0.23 g, 43%) was prepared as a viscous oil: MS (ES) m/e 178 (M+H)+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07741339B2 |
| Quelldatensatz | uspto-grants-2010_06 |
| ORD ID | ord-ff2ee5770f174403ba474c3949bbf8f4 |
| Quellennotiz | uspto-grants-2010_06 |