HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethyl indole-2-carboxylate → 5-fluoro-1-methyl-1H-indole-3-carbaldehyde
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethyl indole-2-carboxylate | HCID 73125 | — |
| Edukt | 5-fluoro-1H-indole-3-carbaldehyde | HCID 259089 | — |
| Produkt | 5-fluoro-1-methyl-1H-indole-3-carbaldehyde | HCID 1382009 | 50% |
Reaktionsschritte
According to the procedure of Preparation 9 (a), except substituting 5-fluoro-1H-indole-3-carboxaldehyde (0.3 g, 1.8 mmole) for the ethyl indole-2-carboxylate, the title compound (0.16 g, 50%) was prepared as a viscous oil: MS (ES) m/e 178 (M+H)+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07741339B2 |
| Quelldatensatz | uspto-grants-2010_06 |
| ORD ID | ord-5cd2d2d17bfe4ed9822fbbe00a15a149 |
| Quellennotiz | uspto-grants-2010_06 |