HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzoyl Peroxide → Methyl 2-bromo-6-(bromomethyl)benzoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzoyl Peroxide | HCID 7187 | — |
| Edukt | N-bromobutanimide | HCID 67184 | — |
| Edukt | Methyl 2-bromo-6-methylbenzoate | HCID 11564857 | — |
| Lösungsmittel | Carbon Tetrachloride | HCID 5943 | — |
| Produkt | Methyl 2-bromo-6-(bromomethyl)benzoate | HCID 23574705 | — |
Reaktionsbedingungen
| Temperatur | 80 °C |
|---|
Reaktionsschritte
2-Bromo-6-methyl-benzoic acid methyl ester (21.8 mmol), and N-bromosuccinimide (21.8 mmol), benzoyl peroxide (1.1 mmol) were combined in 50 mL carbontetrachloride and heated to 80° C. overnight. The resulting precipitate was filtered off, and filtrate concentrated to an oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07049318B2 |
| Quelldatensatz | uspto-grants-2006_05 |
| ORD ID | ord-04167b4522244ba8b1d2d3b4c4e95255 |
| Quellennotiz | uspto-grants-2006_05 |