HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethyl indole-2-carboxylate → 4-fluoro-1-methyl-1H-indole-3-carbaldehyde
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethyl indole-2-carboxylate | HCID 73125 | — |
| Edukt | 4-Fluoro-1H-indole-3-carbaldehyde | HCID 22139006 | — |
| Produkt | 4-fluoro-1-methyl-1H-indole-3-carbaldehyde | HCID 22138994 | 54% |
Reaktionsschritte
According to the procedure of Preparation 9 (a), except substituting 4-fluoro-1H-indole-3-carboxaldehyde (0.41 g, 2.5 mmole) for the ethyl-indole-2-carboxylate, the title compound (0.24 g, 54%) was prepared as a viscous oil: MS (ES) m/e 178 (M+H)+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07741339B2 |
| Quelldatensatz | uspto-grants-2010_06 |
| ORD ID | ord-d928788cda6740eb8747d4e943ef233e |
| Quellennotiz | uspto-grants-2010_06 |