Skatole → 7-chloro-1-methyl-1H-indole
Reaktionsgleichung
[Cl:1][C:2]1[CH:3]=[CH:4][CH:5]=[C:6]2[C:10]=1[NH:9][CH:8]=[CH:7]2.[CH3:11]C1C2C(=CC=CC=2)NC=1>>[Cl:1][C:2]1[CH:3]=[CH:4][CH:5]=[C:6]2[C:10]=1[N:9]([CH3:11])[CH:8]=[CH:7]2Komponenten
3
Versuchsvorschrift
According to the procedure of Preparation 13 (a), except substituting 7-chloroindole for the 3-methylindole, the title compound (2.2 g, 100%) was obtained as a white solid: MS (ES) m/e 166.2 (M+H)+.
Quellen und Nachweise
- ORD-Eintrag
- ord-e8f8388971ae40ecb68578a66714fe8a
- Quelldatensatz
- uspto-grants-2010_06
- Patentnummer
- US07741339B2
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