Skatole → 5-Chloro-1-methylindole
Reaktionsgleichung
[Cl:1][C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][CH:10]=1)[NH:7][CH:6]=[CH:5]2.[CH3:11]C1C2C(=CC=CC=2)NC=1>>[Cl:1][C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][CH:10]=1)[N:7]([CH3:11])[CH:6]=[CH:5]2Komponenten
3
Versuchsvorschrift
According to the procedure of Preparation 13 (a), except substituting 5-chloroindole for the 3-methylindole, the title compound (2.0 g, 91%) was obtained as an amber oil: MS (ES) m/e 166.0 (M+H)+.
Quellen und Nachweise
- ORD-Eintrag
- ord-4b4f53c46a0e4246b4efa366e3273217
- Quelldatensatz
- uspto-grants-2010_06
- Patentnummer
- US07741339B2
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