4-tert-Butylcyclohexanol → 4-Tert-butylcyclohex-1-ene

HRID 1828330

Reaktionsgleichung

Reaktionsgleichung von HRID 1828330
[C:1]([CH:5]1[CH2:10][CH2:9][CH:8](O)[CH2:7][CH2:6]1)([CH3:4])([CH3:3])[CH3:2].OS([O-])(=O)=O.[K+].C(OC(=O)C)C.OS([O-])(=O)=O.[K+]>>[C:1]([CH:5]1[CH2:10][CH2:9][CH:8]=[CH:7][CH2:6]1)([CH3:4])([CH3:3])[CH3:2]

Komponenten

4

Edukt 3

HCID 73914-tert-ButylcyclohexanolHCID 516920Potassium bisulfateHCID 86585043ethylacetate KHSO4

Produkt 1

HCID 166884-Tert-butylcyclohex-1-ene

Reaktionsbedingungen

Temperatur
95 °C

Versuchsvorschrift

20 g 4-t-butyl-1-cyclohexanol are mixed with 17 g KHSO4 and stirred for one week at 95° C. After the addition of ethylacetate KHSO4 is filtered off. Ethylacetate is evaporated and the product obtained by fractional distillation.

Aufarbeitung

  1. filtrationis filtered off
  2. customEthylacetate is evaporated
  3. customthe product obtained by fractional distillation

Quellen und Nachweise

ORD-Eintrag
ord-af0b71c7642b4961a781a860d53df6c6
Quelldatensatz
uspto-grants-2006_06
Patentnummer
US07057059B2

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