Skatole → 4-Chloro-1-methyl-1H-indole
Reaktionsgleichung
[Cl:1][C:2]1[CH:10]=[CH:9][CH:8]=[C:7]2[C:3]=1[CH:4]=[CH:5][NH:6]2.[CH3:11]C1C2C(=CC=CC=2)NC=1>>[Cl:1][C:2]1[CH:10]=[CH:9][CH:8]=[C:7]2[C:3]=1[CH:4]=[CH:5][N:6]2[CH3:11]Komponenten
3
Versuchsvorschrift
According to the procedure of Preparation 13 (a), except substituting 4-chloroindole for the 3-methylindole, the title compound (2.2 g, 100%) was obtained as an amber oil: MS (ES) m/e 166.0 (M+H)+.
Quellen und Nachweise
- ORD-Eintrag
- ord-9ecece90d71f49e38ad0702522d1c7ad
- Quelldatensatz
- uspto-grants-2010_06
- Patentnummer
- US07741339B2
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