HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Carbamic chloride, N-methyl-N-phenyl- → Methyl-phenyl-carbamic acid 4-(5-trifluoromethylpyridin-2-yloxy)-phenyl ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| Edukt | 4-(5-Trifluoromethyl-pyridin-2-yloxy)-phenol | HCID 155241 | — |
| Produkt | Methyl-phenyl-carbamic acid 4-(5-trifluoromethylpyridin-2-yloxy)-phenyl ester | HCID 10150601 | — |
Reaktionsschritte
The title compound was prepared from 4-(5-trifluoromethyl-pyridin-2-yloxy)-phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was purified by preparative HPLC (36%, white crystals). HPLC-MS m/z=389.1 (M+1), Rt: 5.13 min.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07067517B2 |
| Quelldatensatz | uspto-grants-2006_06 |
| ORD ID | ord-ac2b8a1458554d74b7f7c2d87439d629 |
| Quellennotiz | uspto-grants-2006_06 |