2-Butanamine, 1-methoxy- → [4-(2,4-Dichloro-phenyl)-3-nitro-pyridin-2-yl]-(1-methoxymethyl-propyl)-amine

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	2-Butanamine, 1-methoxy-	HCID 93837	—
Edukt	2-Chloro-4-(2,4-dichloro-phenyl)-3-nitro-pyridine	HCID 22052102	—
Produkt	[4-(2,4-Dichloro-phenyl)-3-nitro-pyridin-2-yl]-(1-methoxymethyl-propyl)-amine	HCID 22052219	88%

Reaktionsschritte

2-Chloro-4-(2,4-dichloro-phenyl)-3-nitro-pyridine (0.20 g, 0.66 mmol) and 1-methoxymethyl-propylamine (0.14 g, 1.32 mmol) were treated as in Part D of Example 9 to yield 0.21 g (88%) of [4-(2,4-dichloro-phenyl)-3-nitro-pyridin-2-yl]-(1-methoxymethyl-propyl)-amine: MS (AP) m/z 370.2 [(M+H)+, 97].

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US07067658B2
Quelldatensatz	uspto-grants-2006_06
ORD ID	ord-0cb88146fb7d431c84f6f9f0b98a05c9
Quellennotiz	uspto-grants-2006_06