HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetamidine monohydrochloride → HCID 54283790, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetamidine monohydrochloride | HCID 67170 | — |
| Edukt | Phosphinecarboxylic acid, 1,1-diethoxy-, methyl ester, 1-oxide | HCID 170573 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | HCID 54283790 | HCID 54283790 | — |
Reaktionsschritte
A solution of 98 parts of diethyl methoxycarbonylphosphonate plus 47 parts of acetamidine hydrochloride in 1000 parts of anhydrous tetrahydrofuran can be refluxed for 8 hours and the solvent then removed under reduced pressure to give diethyl 1-amino-1-methylmethyleneaminocarbonylphosphonate. In a similar manner, starting with the appropriate alkoxycarbonylphosphonate and imino compounds, the following compounds can be prepared:
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04066434 |
| Quelldatensatz | uspto-grants-1978_01 |
| ORD ID | ord-86fc9fb571a944cbafec8910d46961a9 |
| Quellennotiz | uspto-grants-1978_01 |