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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1833287Erstellt: 26. Oktober 2026

Acetamidine monohydrochloride → HCID 54283790, Verbindung

https://huagongshe.com/reaction/1833287

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktAcetamidine monohydrochlorideHCID 67170—
EduktPhosphinecarboxylic acid, 1,1-diethoxy-, methyl ester, 1-oxideHCID 170573—
LösungsmittelTetrahydrofuranHCID 8028—
ProduktHCID 54283790HCID 54283790—

Reaktionsschritte

A solution of 98 parts of diethyl methoxycarbonylphosphonate plus 47 parts of acetamidine hydrochloride in 1000 parts of anhydrous tetrahydrofuran can be refluxed for 8 hours and the solvent then removed under reduced pressure to give diethyl 1-amino-1-methylmethyleneaminocarbonylphosphonate. In a similar manner, starting with the appropriate alkoxycarbonylphosphonate and imino compounds, the following compounds can be prepared:

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04066434
Quelldatensatzuspto-grants-1978_01
ORD IDord-86fc9fb571a944cbafec8910d46961a9
Quellennotizuspto-grants-1978_01