3-(3-Nitro-phenyl)-acrylonitrile → HCID 22186098, Verbindung

Beteiligte Stoffe

Reaktionsbedingungen

Reaktionsschritte

There are introduced into a cylinder 3 g of the product obtained in Step 1, 1.59 g of tris(triphenylphosphine)rhodium(I) chloride and 90 ml of benzene. The whole is heated for 5 hours at 40° C. under a hydrogen pressure of 5 bar. The solvent is evaporated off and the residue is purified by chromatography on silica gel using dichloromethane as eluant.

Herkunft & Nachweise