HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Uracil → Benzyl chloromethyl ether
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Uracil | HCID 1174 | — |
| Edukt | 7-Methylxanthine | HCID 68374 | — |
| Edukt | 2-Chloromethyl 2-(trimethylsilyl)ethyl ether | HCID 2724271 | — |
| Produkt | Benzyl chloromethyl ether | HCID 137983 | — |
Reaktionsschritte
In a similar manner to the procedures described in Reference Example 3, reactions were carried out using 7-methylxanthine, instead of pyrimidine-2,4-dione, and using 2-(trimethylsilyl)ethoxymethyl chloride, instead of benzyloxymethyl chloride, to give the title compound (yield 69%) as a pale yellow powder.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06673804B1 |
| Quelldatensatz | uspto-grants-2004_01 |
| ORD ID | ord-aabbc1fe7b634686ad862928f82d70f5 |
| Quellennotiz | uspto-grants-2004_01 |