1,4-Dibromopentane → HCID 68615812, Verbindung
Reaktionsgleichung
[C:1]([O:5][C:6](=[O:16])[N:7]([C:9]1[CH:14]=[CH:13][C:12]([OH:15])=[CH:11][CH:10]=1)[CH3:8])([CH3:4])([CH3:3])[CH3:2].[Br:17][CH2:18][CH2:19][CH2:20][CH:21](Br)[CH3:22]>>[C:1]([O:5][C:6](=[O:16])[N:7]([C:9]1[CH:10]=[CH:11][C:12]([O:15][CH2:22][CH2:21][CH2:20][CH2:19][CH2:18][Br:17])=[CH:13][CH:14]=1)[CH3:8])([CH3:4])([CH3:2])[CH3:3]Komponenten
3
Versuchsvorschrift
In analogy to example 1.4, reaction of (4-Hydroxy-phenyl)-methyl-carbamic acid tert-butyl ester with 1,4-dibromopentane yielded [4-(5-Bromo-pentyloxy)-phenyl]-methyl-carbamic acid tert-butyl ester, MS: 372 (MH+, 1Br).
Quellen und Nachweise
- ORD-Eintrag
- ord-1acfdd86af554af38ba8190daf964897
- Quelldatensatz
- uspto-grants-2004_01
- Patentnummer
- US06683201B2
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